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(Dimethoxythiophosphinoylthio)acetic acid methyl ester

Methyl[(Dimethoxyphosphinothioyl)thio]acetate

CAS: 757-86-8

Molecular Formula: C5H11O4PS2

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(Dimethoxythiophosphinoylthio)acetic acid methyl ester - Names and Identifiers

Name Methyl[(Dimethoxyphosphinothioyl)thio]acetate
Synonyms DIMETHOICACID,METHYLESTER
METHYL (DIMETHOXYPHOSPHINOTHIOYLTHIO)-ACETATE
Methyl[(Dimethoxyphosphinothioyl)thio]acetate
Methyl ((dimethoxyphosphinothioyl)thio)acetate
O,O-DIMETHYL-S-(METHOXY-CARBONYLMETHYL)DITHIOPHOSPHATE
(Dimethoxythiophosphinoylthio)acetic acid methyl ester
O,O-Dimethyl S-methoxy-carbonyl methylphosphorodithioate
[(Dimethoxyphosphinothioyl)thio]acetic acid methyl ester
ACETICACID,(DIMETHOXY-PHOSPHINOTHIONYL)-THIOL-METHYLESTER
Dithiophosphoric acid O,O-dimethyl S-(methoxycarbonyl)methyl ester
CAS 757-86-8
EINECS 212-058-6
InChI InChI=1/C3H6O2S.C2H7O2PS2/c1-5-3(4)2-6;1-3-5(6,7)4-2/h6H,2H2,1H3;1-2H3,(H,6,7)/p-1

(Dimethoxythiophosphinoylthio)acetic acid methyl ester - Physico-chemical Properties

Molecular FormulaC5H11O4PS2
Molar Mass230.24
Physical and Chemical PropertiesChemical properties The pure sulfur phosphate ester is a colorless transparent liquid, m.p.85 ℃/1.3Pa, B. p.125 ~ 132 ℃/53~67Pa, insoluble in water, petroleum ether, soluble in organic solvents such as alcohol, benzene, ketone, etc. Industrial products are light yellow transparent liquid with relative density of 1.29~1.30(20 ℃).
UseUses O,O dimethyl-S-(methoxycarbonylmethyl) dithiophosphate, short for thiophosphate, is an intermediate of The organophosphorus pesticide Dimethoate.

(Dimethoxythiophosphinoylthio)acetic acid methyl ester - Upstream Downstream Industry

Raw MaterialsDimethyl sulfide
Methyl chloroacetate
Downstream ProductsDimethoate
O,O-DIMETHYL-S-(METHOXY-CARBONYL) THIOPHOSPHATE

(Dimethoxythiophosphinoylthio)acetic acid methyl ester - Nature

Open Data Verified Data

colorless liquid with malodorous odor. Density 1.29g/cm3. Boiling point of 65 degrees C (2kPa).

Last Update:2024-01-02 23:10:35

(Dimethoxythiophosphinoylthio)acetic acid methyl ester - Preparation Method

Open Data Verified Data

from chloroacetic acid methyl ester and sulfide ammonium salt (O,0 'dimethyl dithiophosphate ammonium) synthesis. The crude product obtained from the synthesis was distilled under reduced pressure to obtain a finished product.

Last Update:2022-01-01 10:38:12

(Dimethoxythiophosphinoylthio)acetic acid methyl ester - Use

Open Data Verified Data

pesticide intermediates. Mainly used for the preparation of dimethoate, malathion and other organophosphorus pesticides.

Last Update:2022-01-01 10:38:11

(Dimethoxythiophosphinoylthio)acetic acid methyl ester - Safety

Open Data Verified Data

This product is toxic. Has a stimulating effect on the skin. Production process should pay attention to prevent material leakage, avoid contact with the human body. Operators should wear protective equipment. Packaged in iron or plastic barrels. Store in a cool, ventilated, dry warehouse. Pay attention to fire prevention, and store and transport toxic substances according to regulations.

Last Update:2022-01-01 10:38:12

(Dimethoxythiophosphinoylthio)acetic acid methyl ester - Production method

The preparation method is to react methyl sulfide ammonium salt with methyl chloroacetate to obtain sulfur phosphate ester.
1100~1200kg of methyl sulfide ammonium salt aqueous solution (content about 38% ~ 42%) and a certain amount of methyl chloroacetate are put into a reaction kettle, stirred, pH = 6~7 is adjusted, then the temperature is raised to 35~38 ℃, the heating is stopped, the temperature is raised by itself, and the temperature is controlled at 55~58 ℃ for 2.5h. After the reaction, cool, add 200kg of water, stir for a moment, and pump the reaction liquid to the water separator to stand and delaminate. After the ester layer is filtered, it is allowed to stand for 30min in a water separator with 200kg of water added in advance, and the waste water is separated. After the ester layer is washed with water and standing, crude sulfur and phosphorus esters are obtained. Crude sulfur and phosphorus esters are desolated by a rising film evaporator, separated by gas and liquid, and cooled to obtain refined sulfur and phosphorus esters.

Last Update:2024-04-10 22:29:15
(Dimethoxythiophosphinoylthio)acetic acid methyl ester
Supplier List
Shanghai Yuanye Bio-Technology Co., Ltd.
Product Name: Methyl [(dimethoxyphosphinothioyl)thio]acetate Visit Supplier Webpage Request for quotation
CAS: 757-86-8
Tel: 18301782025
Email: 3008007409@qq.com
Mobile: 18021002903
QQ: 3008007409 Click to send a QQ message
Shanghai Yuanye Bio-Technology Co., Ltd.
Product Name: Methyl [(dimethoxyphosphinothioyl)thio]acetate Visit Supplier Webpage Request for quotation
CAS: 757-86-8
Tel: 18301782025
Email: 3008007409@qq.com
Mobile: 18021002903
QQ: 3008007409 Click to send a QQ message
View History
(Dimethoxythiophosphinoylthio)acetic acid methyl ester
1-[(4-methoxy-3-nitrophenyl)methyl]hydrazine
1-[3,5-bis(trifluoromethyl)phenyl]-2-bromoethanone
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Perfluorotributylamine
4-MORPHOLINYL-2-BENZOTHIAZYLDISULPHIDE
(Z)-2-(2,4-二氧代-3-丙基噻唑烷-5-基亚基)乙酸
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tris((trimethoxysilyl)propyl)isocyanurate
(3-甲氧基-4-甲基苯基)甲醇
Raw Materials for (Dimethoxythiophosphinoylthio)acetic acid methyl ester
Dimethyl sulfide
Methyl chloroacetate
Downstream Products for (Dimethoxythiophosphinoylthio)acetic acid methyl ester
Dimethoate
O,O-DIMETHYL-S-(METHOXY-CARBONYL) THIOPHOSPHATE
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